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https://scholarhub.balamand.edu.lb/handle/uob/2638| Title: | Tetradecanuclear iron(III)-oxo nanoclusters stabilized by trilacunary heteropolyanions | Authors: | Ibrahim, Masooma Haider, Ali Xiang, Y Bassil, Bassem Carey, Akina M. Rullik, L Jameson, G.B Doungmene, F Mbomekallé, I.M De Oliveira, P Mereacre, V Kostakis, G.E Powell, A.K Kortz, Ulrich |
Affiliations: | Department of Chemistry | Issue Date: | 2015 | Part of: | Journal of inorganic chemistry | Volume: | 54 | Issue: | 13 | Start page: | 6136 | End page: | 6146 | Abstract: | The tetrameric, multi-Fe(III)-containing polyoxotungstates [Fe14O6(OH)13(P2W15O56)4](31-) (1) and [Na2Fe14(OH)12(PO4)4(A-α-XW9O34)4](20-) (X = Si(IV) (2), Ge(IV) (3)) have been successfully synthesized under conventional reaction conditions in aqueous, slightly acidic (1), or basic (2 and 3) media. Polyanions 1-3 were characterized in the solid state by single-crystal X-ray diffraction, IR spectroscopy, thermogravimetric analysis, and magnetic studies, and in solution by electrochemistry. |
URI: | https://scholarhub.balamand.edu.lb/handle/uob/2638 | Type: | Journal Article |
| Appears in Collections: | Department of Chemistry |
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