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UOB Libraries created the UOBScholar Hub, an Institutional Repository (IR) for archiving and collecting all the research output of the UOB community. It aims to improve the visibility, usage and impact of research conducted at UOB. Materials included are: academic journal articles, conference papers and presentations, books and book chapters, ongoing research papers, reports and patents.
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https://scholarhub.balamand.edu.lb/handle/uob/2077| DC Field | Value | Language |
|---|---|---|
| dc.contributor.author | Allouch, Ahmad | en_US |
| dc.contributor.author | Hassan, Inas EL | en_US |
| dc.contributor.author | Zeine, Abdel Razzak El | en_US |
| dc.contributor.author | Abou Dalle, Adib | en_US |
| dc.contributor.author | Bouchkara, Mohammad | en_US |
| dc.contributor.author | Nakat, Hanna El | en_US |
| dc.contributor.author | Omar, Fawaz El | en_US |
| dc.date.accessioned | 2020-12-23T09:05:52Z | - |
| dc.date.available | 2020-12-23T09:05:52Z | - |
| dc.date.issued | 2012 | - |
| dc.identifier.uri | https://scholarhub.balamand.edu.lb/handle/uob/2077 | - |
| dc.description.abstract | The separation of racemic-N-[(2Z)-4-methyl-3-(2-methylphenyl)-1,3-thiazol-2(3H)-ylidene]-N- (2-chloro-4-nitrophenyl)amine, which belongs to the 2-aryl-imino-N-(2-aryl)-thiazoline family, to collect its atropisomers, was studied using reversed-phase high-performance liquid chromatography (RP-HPLC) with hydroxypropyl-gamma-cyclodextrin (HP-γ-CD) as a complexing additive to the racemic mixture (to obtain chiral molecules) and hexane-propan-2-ol as a mobile phase. The effects of mobile phase composition, concentration of HP-γ-CD and time of incubation of the CD-substrate on separation were systematically investigated to establish the optimum resolution conditions. | en_US |
| dc.format.extent | 8 p. | en_US |
| dc.language.iso | eng | en_US |
| dc.subject | 2-aryl-imino-N-(2-aryl)-thiazoline | en_US |
| dc.subject | HP−γ-CD | en_US |
| dc.subject | HPLC | en_US |
| dc.subject | Atropisomeric separation | en_US |
| dc.title | HPLC separaton of hydrophobic atropisomers | en_US |
| dc.type | Journal Article | en_US |
| dc.contributor.affiliation | Department of Chemistry | en_US |
| dc.description.volume | 10 | en_US |
| dc.description.issue | 2 | en_US |
| dc.description.startpage | 799 | en_US |
| dc.description.endpage | 807 | en_US |
| dc.date.catalogued | 2019-07-04 | - |
| dc.description.status | Published | en_US |
| dc.identifier.OlibID | 192710 | - |
| dc.relation.ispartoftext | International journal of chemical sciences | en_US |
| dc.provenance.recordsource | Olib | en_US |
| crisitem.author.parentorg | Faculty of Arts and Sciences | - |
| Appears in Collections: | Department of Chemistry | |
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