Please use this identifier to cite or link to this item: https://scholarhub.balamand.edu.lb/handle/uob/2077
DC FieldValueLanguage
dc.contributor.authorAllouch, Ahmaden_US
dc.contributor.authorHassan, Inas ELen_US
dc.contributor.authorZeine, Abdel Razzak Elen_US
dc.contributor.authorAbou Dalle, Adiben_US
dc.contributor.authorBouchkara, Mohammaden_US
dc.contributor.authorNakat, Hanna Elen_US
dc.contributor.authorOmar, Fawaz Elen_US
dc.date.accessioned2020-12-23T09:05:52Z-
dc.date.available2020-12-23T09:05:52Z-
dc.date.issued2012-
dc.identifier.urihttps://scholarhub.balamand.edu.lb/handle/uob/2077-
dc.description.abstractThe separation of racemic-N-[(2Z)-4-methyl-3-(2-methylphenyl)-1,3-thiazol-2(3H)-ylidene]-N- (2-chloro-4-nitrophenyl)amine, which belongs to the 2-aryl-imino-N-(2-aryl)-thiazoline family, to collect its atropisomers, was studied using reversed-phase high-performance liquid chromatography (RP-HPLC) with hydroxypropyl-gamma-cyclodextrin (HP-γ-CD) as a complexing additive to the racemic mixture (to obtain chiral molecules) and hexane-propan-2-ol as a mobile phase. The effects of mobile phase composition, concentration of HP-γ-CD and time of incubation of the CD-substrate on separation were systematically investigated to establish the optimum resolution conditions.en_US
dc.format.extent8 p.en_US
dc.language.isoengen_US
dc.subject2-aryl-imino-N-(2-aryl)-thiazolineen_US
dc.subjectHP−γ-CDen_US
dc.subjectHPLCen_US
dc.subjectAtropisomeric separationen_US
dc.titleHPLC separaton of hydrophobic atropisomersen_US
dc.typeJournal Articleen_US
dc.contributor.affiliationDepartment of Chemistryen_US
dc.description.volume10en_US
dc.description.issue2en_US
dc.description.startpage799en_US
dc.description.endpage807en_US
dc.date.catalogued2019-07-04-
dc.description.statusPublisheden_US
dc.identifier.OlibID192710-
dc.relation.ispartoftextInternational journal of chemical sciencesen_US
dc.provenance.recordsourceOliben_US
Appears in Collections:Department of Chemistry
Show simple item record

Record view(s)

7
checked on Oct 7, 2022

Google ScholarTM

Check


Items in DSpace are protected by copyright, with all rights reserved, unless otherwise indicated.